1: p-bromophenyl bromide With tert.-butyl lithium in tetrahydrofuran; pentane
T=-78 - 20°C; Inert atmosphere;
2: selenium in tetrahydrofuran; pentane
T=20°C; 0.5 h; Inert atmosphere;
3: methyl iodide in tetrahydrofuran; pentane
T=20°C; 1 h; Inert atmosphere;
参考文献
Park, Young S.; Widawsky, Jonathan R.; Kamenetska, Maria; Steigerwald, Michael L.; Hybertsen, Mark S.; Nuckolls, Colin; Venkataraman, Latha
Journal of the American Chemical Society, 2009 , vol. 131, # 31 p. 10820 - 10821