1.1: N-bromosuccinmide / chloroform / 8 h / 40 °C
2.1: sec.-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere
2.2: 24 h / -78 - 20 °C / Inert atmosphere
View Scheme
参考文献
Idzik, Krzysztof Ryszard; Cywinski, Piotr J.; Cranfield, Charles G.; Mohr, Gerhard J.; Beckert, Rainer
Journal of Fluorescence, 2011 , vol. 21, # 3 p. 1195 - 1204