[[(Z)-1-丙烯基]磺酰基]苯合成路线 （共 11 条）
反应条件
[Pd((p-methoxyphenyl)-BIAN)(dimethyl fumarate)]; hydrogen in tetrahydrofuran
T=20°C; P=760 Torr; 24 h;
参考文献
Guo, Hao; Zheng, Zilong; Yu, Fei; Ma, Shengming; Holuigue, Alexandre; Tromp, Dorette S.; Elsevier, Cornelis J.; Yu, Yihua
Angewandte Chemie - International Edition, 2006 , vol. 45, # 30 p. 4997 - 5000
反应条件
in isopropyl alcohol
at 15 °C, 3 h; GLC;
参考文献
Ryu,Ilhyong; Kusumoto, Nobuo; Ogawa, Akiya; Kambe, Nobuaki; Sonoda, Noboru
Organometallics, 1989 , vol. 8, p. 2279 - 2281
反应条件
trifluorormethanesulfonic acid in toluene
T=27°C; 12 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Funk, Raymond L.; Umstead-Daggett, Joy; Brummond, Kay M.
Tetrahedron Letters, 1993 , vol. 34, # 18 p. 2867 - 2870
反应条件
in isopropyl alcohol
at 15 °C, 6 h; GLC;
参考文献
Ryu,Ilhyong; Kusumoto, Nobuo; Ogawa, Akiya; Kambe, Nobuaki; Sonoda, Noboru
Organometallics, 1989 , vol. 8, p. 2279 - 2281
反应条件
in isopropyl alcohol
at 15 °C, 6 h; GLC;
参考文献
Ryu,Ilhyong; Kusumoto, Nobuo; Ogawa, Akiya; Kambe, Nobuaki; Sonoda, Noboru
Organometallics, 1989 , vol. 8, p. 2279 - 2281
反应条件
aluminum oxide
2 h; Irradiation;
参考文献
Villemin, Didier; Alloum, Abdelkrim Ben
Synthetic Communications, 1990 , vol. 20, # 7 p. 925 - 932
反应条件
1: 1.) n-BuLi / 1.) THF, O deg C, 10 min, 2.) -78 deg C
2: triflic acid / toluene / 12 h / 27 °C
View Scheme
参考文献
Funk, Raymond L.; Umstead-Daggett, Joy; Brummond, Kay M.
Tetrahedron Letters, 1993 , vol. 34, # 18 p. 2867 - 2870
反应条件
1: 82 percent / dimethylformamide
2: 1.) n-BuLi / 1.) THF, O deg C, 10 min, 2.) -78 deg C
3: triflic acid / toluene / 12 h / 27 °C
View Scheme
参考文献
Funk, Raymond L.; Umstead-Daggett, Joy; Brummond, Kay M.
Tetrahedron Letters, 1993 , vol. 34, # 18 p. 2867 - 2870
反应条件
in methanol
at 25 °C, 6 h; PTLC, determination by GLC;
参考文献
Ryu,Ilhyong; Kusumoto, Nobuo; Ogawa, Akiya; Kambe, Nobuaki; Sonoda, Noboru
Organometallics, 1989 , vol. 8, p. 2279 - 2281
反应条件
in dimethyl sulfoxide
T=24.9°C; ΔG(excit.), ΔH(excit.), ΔS(excit.); Thermodynamic data;
参考文献
Kimmelma, Reijo
Acta Chemica Scandinavica, 1993 , vol. 47, # 12 p. 1201 - 1206
