1-(3-羟基-5,6,7,8-四氢-2-萘)-乙酮合成路线 （共 9 条）
反应条件
acetic acid; TiCl4 in ethyl acetate
参考文献
Zaveri, Nurulain; Chao, Wan-Ru
Patent: US2004/29914 A1, 2004 ;
反应条件
zirconium tetrachloride in dichloromethane 48 h; Ambient temperature;
参考文献
Harrowven, David C.; Dainty, Richard F.
Tetrahedron Letters, 1996 , vol. 37, # 42 p. 7659 - 7660
反应条件
aluminium trichloride in dichloromethane 2 h; Ambient temperature;
参考文献
Einhorn; Demerseman; Rene; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 1 p. 79 - 84
反应条件
1: 5,6,7,8-tetrahydro-2-hydroxy naphthalene With titanium tetrachloride T=20°C; 2: acetyl chloride T=20 - 120°C; 1.25 h;
参考文献
Bensari, Ahlem; Zaveri, Nurulain T.
Synthesis, 2003 , # 2 p. 267 - 271
反应条件
toluene-4-sulfonic acid in toluene 2 h; Reflux;
参考文献
J'mour, Asma; Rezgui, Farhat
Journal of Chemical Research, 2009 , # 10 p. 642 - 644
反应条件
1: 32 percent / SnCl4 / benzene / 3 h / Ambient temperature 2: 93 percent / AlCl3 / CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
Einhorn; Demerseman; Rene; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 1 p. 79 - 84
反应条件
1: 64 g / pyridine / CH2Cl2 / 2 h / 20 °C 2: 66 percent / AlCl3 / various solvent(s) / 5 h / 100 °C View Scheme
参考文献
Bolchi, Cristiano; Catalano, Paolo; Fumagalli, Laura; Gobbi, Marco; Pallavicini, Marco; Pedretti, Alessandro; Villa, Luigi; Vistoli, Giulio; Valoti, Ermanno
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 18 p. 4937 - 4951
反应条件
aluminium trichloride; sulfuric acid; sodium chloride 2.) 170 deg C; Multistep reaction;
参考文献
Begley, Michael J.; Gill, G. Bryon; Pattenden, Gerald; Stapleton, Alan; Raphael, Richard A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1677 - 1684
反应条件
1: 83 percent / K2CO3 / dimethylformamide / 1 h / Heating
2: 40 percent Chromat. / SnCl4, HNO3 (d=1.52) / CH2Cl2 / 1 h / 20 - 30 °C
View Scheme
参考文献
Einhorn; Demerseman; Rene; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 1 p. 79 - 84
