potassium tert-butylate in tetrahydrofuran
T=20°C; Inert atmosphere;
参考文献
THE CURATORS OF THE UNIVERSITY OF MISSOURI; LEE, Jr., Mark Wayne; SEVRYUGINA, Yulia
Patent: WO2013/82150 A1, 2013 ;
Location in patent: Paragraph 0124 ;
1: With n-butyllithium; diisopropylamine in tetrahydrofuran; cyclohexane
T=-78°C; 1 h;
2: With diethyl chlorophosphate in tetrahydrofuran; hexane
T=-78 - 20°C;
参考文献
Busch, Mark; Schlageter, Martin; Weingand, Daniel; Gehring, Timo
Chemistry - A European Journal, 2009 , vol. 15, # 33 p. 8251 - 8258
