1-苄基氮杂丁烷-2-羧酸酰胺合成路线 （共 3 条）
反应条件
ammonium hydroxide 3 h;
参考文献
Starmans, Wim A. J.; Doppen, Roy G.; Thijs, Lambertus; Zwanenburg, Binne
Tetrahedron Asymmetry, 1998 , vol. 9, # 3 p. 429 - 435
反应条件
1: 45 percent / K2CO3 / acetonitrile; H2O / Heating 2: 81 percent / conc. aq. NH3 / 3 h View Scheme
参考文献
Starmans, Wim A. J.; Doppen, Roy G.; Thijs, Lambertus; Zwanenburg, Binne
Tetrahedron Asymmetry, 1998 , vol. 9, # 3 p. 429 - 435
反应条件
borane-THF 1.) THF, a) RT, 2 h, b) reflux, 8 h, 2.) EtOH, reflux, 2 h; Yield given. Multistep reaction;
参考文献
Fujita, Masahiro; Chiba, Katsumi; Tominaga, Yukio; Hino, Katsuhiko
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 5 p. 787 - 796
