1,2,3,4-四-O-乙酰-β-D-吡喃木糖合成路线 (共 16 条)
反应条件
magnesium oxide in methanol 0.416667 h; Ambient temperature; Yield given;
参考文献
Herzig, Jacob; Nudelman, Abraham
Carbohydrate Research, 1986 , vol. 153, p. 162 - 167
反应条件
boron trifluoride diethyl etherate in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Wei, Jinhua; Lv, Xun; Lue, Yang; Yang, Gangzhu; Fu, Lifeng; Yang, Liu; Wang, Jianjun; Gao, Jianhui; Cheng, Shuihong; Duan, Qian; Jin, Cheng; Li, Xuebing
European Journal of Organic Chemistry, 2013 , # 12 p. 2414 - 2419
反应条件
1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / |Inert atmosphere 2: methanol; sodium methylate / 20 °C / pH 10 - 11 View Scheme
参考文献
European Journal of Organic Chemistry, , # 12 p. 2414 - 2419
反应条件
tri-n-butyltin methoxide in methanol T=50°C; 2 h; other catalyst (Bu2SnO); Product distributionRate constant;
参考文献
Herzig, Jacob; Nudelman, Abraham; Gottlieb, Hugo E.
Carbohydrate Research, 1988 , vol. 177, p. 21 - 28
反应条件
4 A molecular sieve; tin(IV) chloride in dichloromethane Product distribution; Further Variations:time;
参考文献
Konstantinovic; Petrovic; Spasojevic; Mojsilovic
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 7 p. 614 - 618
反应条件
anhydrous iron chloride; trimethylsilylazide in dichloromethane
T=20°C; 3 h; Inert atmosphere;
参考文献
Salunke, Santosh B.; Babu, N. Seshu; Chen, Chien-Tien
Chemical Communications, 2011 , vol. 47, # 37 p. 10440 - 10442