(2,2-二氟乙烯基)苯合成路线 （共 44 条）
反应条件
zinc in ethanol
10 h; Heating; Title compound not separated from byproducts;
参考文献
Okano,T.; Ito,K.; Ueda,T.
Journal of Fluorine Chemistry, 1986 , vol. 32, p. 377
反应条件
zinc in ethanol
10 h; Heating; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Okano,T.; Ito,K.; Ueda,T.
Journal of Fluorine Chemistry, 1986 , vol. 32, p. 377
反应条件
sodium iodide in various solvent(s)
Ambient temperature;
参考文献
Burton, Donald J.; Takei, Ryutaro; Shin-Ya, Seiji
Journal of Fluorine Chemistry, 1981 , vol. 18, p. 197 - 202
反应条件
phenyllithium
1.) benzene-ether, triglyme 0 deg C, 1h RT, 2.) 12h RT; Yield given. Multistep reaction;
参考文献
Wheaton, Gregory A.; Burton, Donald J.
Journal of Organic Chemistry, 1983 , vol. 48, # 7 p. 917 - 927
反应条件
tetrakis(triphenylphosphine) palladium(0); zinc
1.) THF, 50-60 deg C, 2.) THF, 60 deg C, 6 h; Yield given. Multistep reaction;
参考文献
Nguyen, Ba V.; Burton, Donald J.
Journal of Organic Chemistry, 1997 , vol. 62, # 22 p. 7758 - 7764
反应条件
tetrakis(triphenylphosphine) palladium(0); zinc
1.) THF, 50-60 deg C, 2.) THF, 60 deg C, 4 h; Yield given. Multistep reaction;
参考文献
Nguyen, Ba V.; Burton, Donald J.
Journal of Organic Chemistry, 1997 , vol. 62, # 22 p. 7758 - 7764
反应条件
in tetrahydrofuran
T=100°C; 4 h; Inert atmosphere;
参考文献
Thomoson, Charles S.; Martinez, Henry; Dolbier Jr., William R.
Journal of Fluorine Chemistry, 2013 , vol. 150, p. 53 - 59
反应条件
hydrogenchloride; acetic acid; zinc
参考文献
Eliseenkov,E.V. et al.
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, p. 781 - 785,721 - 724
反应条件
tetrakis(triphenylphosphine) palladium(0); chloro-trimethyl-silane; diiodomethane; zinc
1.) THF, 60-90 deg C, 30 min, 2.) THF, 60 deg C, 4 h; Yield given. Multistep reaction. Further byproducts given;
参考文献
Nguyen, Ba V.; Burton, Donald J.
Journal of Organic Chemistry, 1997 , vol. 62, # 22 p. 7758 - 7764
反应条件
phenyllithium
1.) benzene-ether, triglyme 0 deg C 1h RT, 2.) 12h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Wheaton, Gregory A.; Burton, Donald J.
Journal of Organic Chemistry, 1983 , vol. 48, # 7 p. 917 - 927
