1: With benzo[1,3,2]dioxaborole; rhodium complex 2 in toluene T=20°C; Addition; Hydroboration; 2 h; 2: With sodium hydroxide; water; dihydrogen peroxide in toluene T=20°C; Oxidation; 2 h; Title compound not separated from byproducts;
参考文献
Moteki, Shin A.; Wu, Di; Chandra, Kusum L.; Sahadeva Reddy; Takacs, James M.
Organic Letters, 2006 , vol. 8, # 14 p. 3097 - 3100
1: in carbon disulfide T=20°C; 5 h; 2: With hydroxylamine-o-sulphonic acid in methanol; carbon disulfide T=0 - 20°C; 12 h; Further stages. Title compound not separated from byproducts.;
参考文献
Ramachandran, P. Veeraraghavan; Madhi, Sateesh; O'Donnell, Martin J.
Journal of Fluorine Chemistry, 2006 , vol. 127, # 9 p. 1252 - 1255
