反应条件
1: (iPrPNN)CoCl2; NaBEt3H / tetrahydrofuran; toluene / 0.25 h / 25 °C / |Inert atmosphere; |Glovebox; |Schlenk technique
2: palladium diacetate; potassium tert-butylate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine / toluene; water / 24 h / 80 °C / |Schlenk technique; |Glovebox; |Inert atmosphere
View Scheme
参考文献
Zhang, Lei; Zuo, Ziqing; Leng, Xuebing; Huang, Zheng
Angewandte Chemie - International Edition, 2014 , vol. 53, # 10 p. 2696 - 2700
Angew. Chem., 2014 , vol. 126, # 10 p. 2734 - 2738,5