in pentane under Ar, equimolar amts. of FcolC6H4CHCH2 and Fe2(CO)9 stirred in pentane at 20°C for 2-3 d; filtered, evapd. at 20°C/1 Torr, chromd. (neutral Al2O3 (activity I), pentane, at 5°C), concd., admixture sepd. by short-path distn. (20°C; 0.001 Torr), crystals purified by crystn. from pentaneat -80°C; elem. anal.;
参考文献
Schmidt, Eckhart K.G.; Dogan, Mehmet
Journal of Organometallic Chemistry, 1982 , vol. 234, # 1 p. 73 - 84
in pentane under Ar, equimolar amts. of FcolC6H4CHCH2 and Fe2(CO)9 stirred in pentane at 20°C for 2-3 d; filtered, evapd. at 20°C/1 Torr, chromd. (neutral Al2O3 (activity I), pentane, at 5°C), concd., admixture sepd. by short-path distn. (20°C; 0.001 Torr), crystals purified by crystn. from pentaneat -80°C; elem. anal.;
参考文献
Schmidt, Eckhart K.G.; Dogan, Mehmet
Journal of Organometallic Chemistry, 1982 , vol. 234, # 1 p. 73 - 84
