反应条件
1: (2,3,4,5,6-pentafluorophenyl)methyl trifluoromethyl sulfone With tert.-butyl lithium in diethyl ether
T=-78°C; 0.5 h;
2: trifluoromethylsulfonic anhydride in diethyl ether
T=-78 - 20°C; 1 h;
参考文献
Ishihara, Kazuaki; Hasegawa, Aiko; Yamamoto, Hisashi
Angewandte Chemie - International Edition, 2001 , vol. 40, # 21 p. 4077 - 4079