2,5-二氯吡啶-3,4-二胺合成路线 （共 6 条）
反应条件
hydrogen; nickel in ethanol
参考文献
Liu; Luo; Mozdziesz; Lin; Dutschman; Gullen; Cheng; Sartorelli
Nucleosides, Nucleotides and Nucleic Acids, 2001 , vol. 20, # 12 p. 1975 - 2000
反应条件
1: 91 percent / TFA; aq. H2O2 / 70 - 75 °C
2: 50.5 percent / conc. H2SO4; KNO3
3: 85 percent / H2 / Raney Ni / ethanol
4: 65 percent / conc. H2SO4; KNO3 / 0 - 20 °C
5: 97 percent / conc. H2SO4 / 20 °C
6: 94 percent / H2 / Raney Ni / ethanol
View Scheme
参考文献
Liu; Luo; Mozdziesz; Lin; Dutschman; Gullen; Cheng; Sartorelli
Nucleosides, Nucleotides and Nucleic Acids, 2001 , vol. 20, # 12 p. 1975 - 2000
反应条件
1: 65 percent / conc. H2SO4; KNO3 / 0 - 20 °C
2: 97 percent / conc. H2SO4 / 20 °C
3: 94 percent / H2 / Raney Ni / ethanol
View Scheme
参考文献
Liu; Luo; Mozdziesz; Lin; Dutschman; Gullen; Cheng; Sartorelli
Nucleosides, Nucleotides and Nucleic Acids, 2001 , vol. 20, # 12 p. 1975 - 2000
反应条件
1: 50.5 percent / conc. H2SO4; KNO3
2: 85 percent / H2 / Raney Ni / ethanol
3: 65 percent / conc. H2SO4; KNO3 / 0 - 20 °C
4: 97 percent / conc. H2SO4 / 20 °C
5: 94 percent / H2 / Raney Ni / ethanol
View Scheme
参考文献
Liu; Luo; Mozdziesz; Lin; Dutschman; Gullen; Cheng; Sartorelli
Nucleosides, Nucleotides and Nucleic Acids, 2001 , vol. 20, # 12 p. 1975 - 2000
反应条件
1: 85 percent / H2 / Raney Ni / ethanol
2: 65 percent / conc. H2SO4; KNO3 / 0 - 20 °C
3: 97 percent / conc. H2SO4 / 20 °C
4: 94 percent / H2 / Raney Ni / ethanol
View Scheme
参考文献
Liu; Luo; Mozdziesz; Lin; Dutschman; Gullen; Cheng; Sartorelli
Nucleosides, Nucleotides and Nucleic Acids, 2001 , vol. 20, # 12 p. 1975 - 2000
反应条件
1: 97 percent / conc. H2SO4 / 20 °C
2: 94 percent / H2 / Raney Ni / ethanol
View Scheme
参考文献
Liu; Luo; Mozdziesz; Lin; Dutschman; Gullen; Cheng; Sartorelli
Nucleosides, Nucleotides and Nucleic Acids, 2001 , vol. 20, # 12 p. 1975 - 2000
