2-乙酰基-1,3-环己二酮合成路线 （共 18 条）
参考文献
Lessel
Archiv der Pharmazie, 1994 , vol. 327, # 9 p. 571 - 579
反应条件
oxalyl dichloride in chloroform 1 h; Heating;
参考文献
Kirchlechner
Chemische Berichte, 1982 , vol. 115, # 7 p. 2461 - 2466
反应条件
palladium on activated charcoal; ethanol Hydrogenation;
参考文献
Journal of the Chemical Society, , p. 803,808
反应条件
1: 90 percent / NH2-NH2 / ethanol / 4 h / Ambient temperature 2: 80 percent / NaBH4 / ethanol / 4 h / 40 °C 3: 85 percent / p-toluenesulfonic acid / 10percent Pd/C / dioxane / 8 h / 100 °C View Scheme
参考文献
Synthesis, , # 11 p. 982 - 983
反应条件
in isopropyl alcohol
反应条件
iodine 9 h; Microwave irradiation;
参考文献
Chemistry - A European Journal, , vol. 19, # 24 p. 7917 - 7930
反应条件
1: With AlCl3, aluminium chloride in anhydrous dichloroethane
T=20°C; 2 h; Inert atmosphere;
2: With sulfuric acid in anhydrous dichloroethane; water
Inert atmosphereCooling with ice;
参考文献
ADDEX PHARMA S.A.; BOLEA, Christelle; SYLVAIN, Celanire
Patent: WO2010/79238 A1, 2010 ;
Location in patent: Page/Page column 31 ;
WO 2010/079238 A1
反应条件
triethylamine in acetonitrile
参考文献
Wojtkowski, Paul Walter
Patent: US2002/49317 A1, 2002 ;
反应条件
Barium in tetrahydrofuran
4 h; Heating;
参考文献
Lim, Sunkwon; Min, Yosep; Choi, Bohyun; Kim, Daesig; Yoon, Il; Lee, Shim Sung; Lee, Ik-Mo
Tetrahedron Letters, 2001 , vol. 42, # 43 p. 7645 - 7649
