2,4-二甲基噻唑-5乙酸乙酯合成路线 （共 9 条）
参考文献
Gregory; Wiggins
Journal of the Chemical Society, 1947 , p. 1400,1402
Full Text Show Details
Burger; Ullyot
Journal of Organic Chemistry, 1947 , vol. 12, p. 342,351
反应条件
1: hydrogenchloride; bromine / water / -5 - 20 °C / Large scale reaction 2: 2 h / Reflux; Large scale reaction View Scheme
参考文献
Guercio, Giuseppe; Castoldi, Damiano; Giubellina, Nicola; Lamonica, Alessandro; Ribecai, Arianna; Stabile, Paolo; Westerduin, Pieter; Dams, Riet; Nicoletti, Anna; Rossi, Sara; Bismara, Claudio; Provera, Stefano; Turco, Lucilla
Organic Process Research and Development, 2010 , vol. 14, # 5 p. 1153 - 1161
反应条件
1: 3-acetylpropionic acid With hydrogenchloride; bromine in water 2: ethanol; ethanethioamide
参考文献
Guercio, Giuseppe; Castoldi, Damiano; Giubellina, Nicola; Lamonica, Alessandro; Ribecai, Arianna; Stabile, Paolo; Westerduin, Pieter; Dams, Riet; Nicoletti, Anna; Rossi, Sara; Bismara, Claudio; Provera, Stefano; Turco, Lucilla
Organic Process Research and Development, 2010 , vol. 14, # 5 p. 1153 - 1161
参考文献
Gregory; Wiggins
Journal of the Chemical Society, 1947 , p. 1400,1402
反应条件
2 h; RefluxLarge scale reaction;
参考文献
Guercio, Giuseppe; Castoldi, Damiano; Giubellina, Nicola; Lamonica, Alessandro; Ribecai, Arianna; Stabile, Paolo; Westerduin, Pieter; Dams, Riet; Nicoletti, Anna; Rossi, Sara; Bismara, Claudio; Provera, Stefano; Turco, Lucilla
Organic Process Research and Development, 2010 , vol. 14, # 5 p. 1153 - 1161
反应条件
potassium hydroxide in methanol T=20°C; Large scale reaction;
参考文献
Guercio, Giuseppe; Castoldi, Damiano; Giubellina, Nicola; Lamonica, Alessandro; Ribecai, Arianna; Stabile, Paolo; Westerduin, Pieter; Dams, Riet; Nicoletti, Anna; Rossi, Sara; Bismara, Claudio; Provera, Stefano; Turco, Lucilla
Organic Process Research and Development, 2010 , vol. 14, # 5 p. 1153 - 1161
反应条件
1: aqueous NH3 2: POCl3 3: Raney nickel; methanol / Hydrogenation View Scheme
参考文献
Burger; Ullyot
Journal of Organic Chemistry, 1947 , vol. 12, p. 342,351
反应条件
1: aqueous NH3
2: POCl3
View Scheme
参考文献
Gregory; Wiggins
Journal of the Chemical Society, 1947 , p. 1400,1402
Full Text Show Details
Burger; Ullyot
Journal of Organic Chemistry, 1947 , vol. 12, p. 342,351
参考文献
Gregory; Wiggins
Journal of the Chemical Society, 1947 , p. 1400,1402
Full Text Show Details
Burger; Ullyot
Journal of Organic Chemistry, 1947 , vol. 12, p. 342,351
