1H-1,2,3-三氮唑-5-甲酸乙酯合成路线 (共 7 条)
反应条件
ammonium acetate in acetic acid T=100°C; 4 h;
参考文献
Sezer, Oezkan; Dabak, Kadir; Akar, Ahmet; Anac, Olcay
Helvetica Chimica Acta, 1996 , vol. 79, # 2 p. 449 - 453
反应条件
trimethylsilylazide T=105°C; 96 h; Inert atmosphere;
参考文献
Chattopadhyay, Buddhadeb; Gevorgyan, Vladimir
Organic Letters, 2011 , vol. 13, # 14 p. 3746 - 3749
反应条件
sodium azide in methanol T=18 - 20°C; 2 h;
参考文献
Anisimova; Berestovitskaya; Berkova; Makarova
Russian Journal of Organic Chemistry, 2007 , vol. 43, # 5 p. 652 - 655
反应条件
trifluoroacetic acid T=65°C; 6.5 h;
参考文献
Buckle, Derek R.; Rockell, Caroline J.M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 627 - 630
反应条件
sodium azide in N,N-dimethyl-formamide 3 h; Ambient temperature;
参考文献
Heinzer; Martin
Helvetica Chimica Acta, 1981 , vol. 64, # 5 p. 1379 - 1386
反应条件
Huisgen 1,3-dipolar cycloaddition; 0.166667 h; Microwave irradiationneat (no solvent);
参考文献
Taherpour, Avat Arman; Kheradmand, Khojasteh
Journal of Heterocyclic Chemistry, 2009 , vol. 46, # 1 p. 131 - 133
参考文献
Yamada et al.
Yakugaku Zasshi, 1957 , vol. 77, p. 452,455
Chem.Abstr., 1957 , p. 14697