二(4-甲氧基苯基)(苯基)甲醇合成路线 （共 34 条）
反应条件
1: 91 percent / anhyd. potassium carbonate / dimethylformamide / 20 h / 130 °C
2: 99 percent / 70percent aq. perchloric acid / tetrahydrofuran; H2O / 1.) 0 deg C, 10 min, 2.) RT, 1 d
View Scheme
参考文献
Huszthy; Bradshaw; Krakowiak; Wang; Dalley
Journal of Heterocyclic Chemistry, 1993 , vol. 30, # 5 p. 1197 - 1207
参考文献
Angeloff; Dubey; Pratviel; Bernadou; Meunier
Chemical Research in Toxicology, 2001 , vol. 14, # 10 p. 1413 - 1420
反应条件
perchloric acid; sodium perchlorate in water; acetonitrile
T=25°C; Deamination; Kinetics; Further Variations:pH-valuesReagentsSolvents;
参考文献
Crugeiras, Juan; Maskill, Howard
Journal of the Chemical Society. Perkin Transactions 2, 1998 , # 9 p. 1901 - 1907
参考文献
Imp. Chem. Ind.
Patent: US1873290 , 1929 ;
Full Text Show Details
Imp. Chem. Ind.
Patent: DE558069 , 1929 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 19, p. 631
Full Text Show Details
Imp. Chem. Ind.
Patent: GB325933 , 1929 ;
反应条件
in tetrahydrofuran
0.833333 h; Heating;
参考文献
Arnett, Edward M.; Flowers II, Robert A.; Ludwig, Richard T.; Meekhof, Alison E.; Walek, Stuart A.
Journal of Physical Organic Chemistry, 1997 , vol. 10, # 7 p. 499 - 513
反应条件
perchloric acid; sodium perchlorate in acetonitrile
T=25°C; Kinetics; Further Variations:pH-values;
参考文献
Canle L, Moises; Clegg, William; Demirtas, Ibrahim; Elsegood, Mark R.J.; Haider, Johanna; Maskill, Howard; Miatt, Peter C.
Journal of the Chemical Society. Perkin Transactions 2, 2001 , # 9 p. 1742 - 1747
反应条件
perchloric acid; sodium perchlorate; water in acetonitrile
T=24.84°C; Kinetics; Concentration;
参考文献
Canle L., Moises; Maskill, Howard
Journal of Physical Organic Chemistry, 2013 , vol. 26, # 12 p. 1016 - 1022
反应条件
aluminium trichloride; sulfuric acid
1.) 2 h; Multistep reaction;
参考文献
Rathore, M.; Rani, P.; Mathur, N. K.; Narang, C. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 7 p. 634 - 635
反应条件
perchloric acid; sodium perchlorate in acetonitrile
T=25°C; Kinetics; Further Variations:Solvents;
参考文献
Canle; Demirtas; Maskill
Journal of the Chemical Society, Perkin Transactions 2, 2001 , # 9 p. 1748 - 1752
参考文献
Kauffmann; Pannwitz
Chemische Berichte, 1912 , vol. 45, p. 771
