4,4'-双甲氧基三苯甲基氯合成路线 （共 132 条）
反应条件
1: sodium hydroxide / tetrahydrofuran; water / 1.5 h / 20 °C 2: 80 °C / Cooling with ice 3: tetrafluoroboric acid / water / 0.67 h / Cooling with ice 4: lithium carbonate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C / Heating View Scheme
参考文献
Hansen, Anders S.; Thalhammer, Armin; El-Sagheer, Afaf H.; Brown, Tom; Schofield, Christopher J.
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 4 p. 1181 - 1184
反应条件
pyridine T=20°C; 1 h;
参考文献
Urata, Hidehito; Hara, Hisafumi; Hirata, Yoshihiro; Ohmoto, Norihiko; Akagi, Masao
Tetrahedron Asymmetry, 2005 , vol. 16, # 17 p. 2908 - 2917
反应条件
pyridine; silver nitrate in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Canadian Journal of Chemistry, , vol. 60, p. 1106 - 1113
反应条件
1: DMAP / pyridine / 1.5 h / 20 °C 2: EtN(iso-Pr)2 / tetrahydrofuran / 2 h / 20 °C View Scheme
参考文献
Ivanov, Sergei A.; Volkov, Eugene M.; Oretskaya, Tatiana S.; Mueller, Sabine
Tetrahedron, 2004 , vol. 60, # 41 p. 9273 - 9281
参考文献
Chen, Yao; Peng, Yingdan; Zhang, Jiancun; Fu, Lei
Nucleosides, Nucleotides and Nucleic Acids, 2008 , vol. 27, # 8 p. 1001 - 1008
反应条件
pyridine; silver nitrate in tetrahydrofuran; N,N-dimethyl-formamide 1 h; Ambient temperature;
参考文献
Canadian Journal of Chemistry, , vol. 60, p. 1106 - 1113
反应条件
1: pyridine; 4-(N,N-dimethlyamino)pyridine; triethylamine / 4 h / 20 °C 2: pyridine / dichloromethane / 0.08 h / 20 °C / Large scale reaction View Scheme
参考文献
Janczyk, Matthaeus; Appel, Bettina; Springstubbe, Danilo; Fritz, Hans-Joachim; Mueller, Sabine
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 8 p. 1510 - 1513
参考文献
Nucleosides, nucleotides and nucleic acids, , vol. 22, # 5-8 p. 1007 - 1009
反应条件
pyridine T=20°C; 1 h;
参考文献
Journal of the American Chemical Society, , vol. 132, # 21 p. 7231 - 7233
反应条件
pyridine 1 h; Ambient temperature;
参考文献
Charubala, R.; Uhlmann, E.; Beiter, A. H.; Pfleiderer, W.
Synthesis, 1984 , # 11 p. 965 - 968
