3-乙酰氨基-3-苯基丙酸合成路线 （共 10 条）
反应条件
sodium hydroxide in water T=40°C; pH=11 - 12; 3 h;
参考文献
Kawasaki, Hisashi; Koyama, Koutaro; Kurokawa, Sachio; Watanabe, Kunihiko; Nakazawa, Masakazu; Izawa, Kunisuke; Nakamatsu, Tsuyoshi
Bioscience, Biotechnology and Biochemistry, 2006 , vol. 70, # 1 p. 99 - 106
反应条件
lithium hydroxide in methanol; water 11 h; Heating;
参考文献
Banerji, Biswadip; Mallesham; Kiran Kumar; Kunwar; Iqbal, Javed
Tetrahedron Letters, 2002 , vol. 43, # 36 p. 6479 - 6483
Title/Abstract Full Text View citing articles Show Details
Reddy, P. Rajamohan; Balraju; Madhavan; Banerji, Biswadip; Iqbal, Javed
Tetrahedron Letters, 2003 , vol. 44, # 2 p. 353 - 356
反应条件
1: ammonium acetate / ethanol / 12 h / |Reflux 2: sodium hydroxide / water / 8 h / 40 °C / pH 11 View Scheme
参考文献
Banerji, Biswadip; Mallesham; Kiran Kumar; Kunwar; Iqbal, Javed
Tetrahedron Letters, 2002 , vol. 43, # 36 p. 6479 - 6483
反应条件
1.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / |Cooling with ice 1.2: 20 °C 2.1: thionyl chloride / 24 h / 20 °C 2.2: 24 h / 0 °C 3.1: Carica papaya lipase / hexane / 45 °C / |Resolution of racemate; |Enzymatic reaction View Scheme
参考文献
European Journal of Organic Chemistry, , # 3 p. 557 - 565
反应条件
1.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / |Cooling with ice 1.2: 20 °C 2.1: thionyl chloride / 24 h / 20 °C 2.2: 24 h / 0 °C 3.1: Carica papaya lipase / hexane / 45 °C / |Resolution of racemate; |Enzymatic reaction View Scheme
参考文献
You, Pengyong; Qiu, Jian; Su, Erzheng; Wei, Dongzhi
European Journal of Organic Chemistry, 2013 , # 3 p. 557 - 565
反应条件
sulfuric acid; nitric acid
参考文献
Rodionow et al.
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 520,524; engl. Ausg. S. 551, 554
反应条件
Tris-HCl buffer in glycerol T=45°C; pH=7.5; 0.5 h;
参考文献
You, Pengyong; Qiu, Jian; Su, Erzheng; Wei, Dongzhi
European Journal of Organic Chemistry, 2013 , # 3 p. 557 - 565
反应条件
Tris-HCl buffer in glycerol T=45°C; pH=7.5; 0.5 h;
参考文献
You, Pengyong; Qiu, Jian; Su, Erzheng; Wei, Dongzhi
European Journal of Organic Chemistry, 2013 , # 3 p. 557 - 565
反应条件
Tris-HCl buffer in glycerol T=45°C; pH=7.5; 0.5 h;
参考文献
You, Pengyong; Qiu, Jian; Su, Erzheng; Wei, Dongzhi
European Journal of Organic Chemistry, 2013 , # 3 p. 557 - 565
反应条件
1.1: dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / |Cooling with ice 1.2: 20 °C 2.1: Carica papaya lipase / hexane / 10 h / 45 °C / |Resolution of racemate; |Enzymatic reaction 3.1: hydrogenchloride / water / 10 h / |Reflux 4.1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 65 °C View Scheme
参考文献
You, Pengyong; Qiu, Jian; Su, Erzheng; Wei, Dongzhi
European Journal of Organic Chemistry, 2013 , # 3 p. 557 - 565
