(S,S)-(-)-双(α-甲苄基)胺盐酸盐合成路线 (共 16 条)
反应条件
sodium tetrahydroborate
参考文献
Clayden, Jonathan; Knowles, Faye E.; Menet, Christel J.
Tetrahedron Letters, 2003 , vol. 44, # 16 p. 3397 - 3400
反应条件
N-[(R)-1-(1-naphthyl)ethyl]carbamoyl-derivatized cyclofructan-6 column in ethanol; n-heptane; trifluoroacetic acid T=20°C; Resolution of racemate;
参考文献
Sun, Ping; Wang, Chunlei; Breitbach, Zachary S.; Zhang, Ying; Armstrong, Daniel W.
Analytical Chemistry, 2009 , vol. 81, # 24 p. 10215 - 10226
反应条件
sodium hydroxide in water; toluene pH=Ca. 10; Large scale;
参考文献
Dunn, Peter J.; Hughes, Michael L.; Searle, Patricia M.; Wood, Albert S.
Organic Process Research and Development, 2003 , vol. 7, # 3 p. 244 - 253
反应条件
N-[(R)-1-(1-naphthyl)ethyl]carbamoyl-derivatized cyclofructan-6 column in ethanol; n-heptane; trifluoroacetic acid T=20°C; Resolution of racemate;
参考文献
Analytical Chemistry, , vol. 81, # 24 p. 10215 - 10226
反应条件
sodium hydroxide in water; toluene pH=Ca. 10; Large scale;
参考文献
Dunn, Peter J.; Hughes, Michael L.; Searle, Patricia M.; Wood, Albert S.
Organic Process Research and Development, 2003 , vol. 7, # 3 p. 244 - 253
反应条件
sodium hydroxide in water; toluene pH=Ca. 10; Large scale;
参考文献
Dunn, Peter J.; Hughes, Michael L.; Searle, Patricia M.; Wood, Albert S.
Organic Process Research and Development, 2003 , vol. 7, # 3 p. 244 - 253