1-甲基-4-硝基-1H-咪唑-5-甲腈合成路线 (共 11 条)
反应条件
sulfuric acid; sodium nitrite T=100°C;
参考文献
Hosmane, Ramachandra S.; Bhan, Anila; Rauser, Michael E.
Heterocycles, 1986 , vol. 24, # 10 p. 2743 - 2748
反应条件
1: H2SO4 / anschliessenden Behandeln mit NaNO2 in H2O 2: SOCl2 4: ethanol; Raney nickel / Hydrogenation View Scheme
参考文献
Journal of the Chemical Society, , p. 751,757
反应条件
1: H2SO4 / anschliessenden Behandeln mit NaNO2 in H2O 2: SOCl2 4: ethanol; Raney nickel / Hydrogenation 5: K2CO3; dioxane View Scheme
参考文献
Mann; Porter
Journal of the Chemical Society, 1945 , p. 751,757
反应条件
1: H2SO4 / anschliessenden Behandeln mit NaNO2 in H2O 2: SOCl2 3: ethanol 4: palladium/charcoal; water; methanol / Hydrogenation.Reagens 4:HCl View Scheme
参考文献
Mann; Porter
Journal of the Chemical Society, 1945 , p. 751,757
反应条件
1: H2SO4 / anschliessenden Behandeln mit NaNO2 in H2O
2: SOCl2
3: ethanol
View Scheme
参考文献
Mann; Porter
Journal of the Chemical Society, 1945 , p. 751,757
反应条件
hydrogen sulfide; diethylamine in N,N-dimethyl-formamide
T=60°C; Addition; reduction; 3 h;
参考文献
Panzica, Raymond P.; Townsend, Leroy B.
Nucleosides and Nucleotides, 1999 , vol. 18, # 11-12 p. 2345 - 2356
反应条件
1: H2SO4 / anschliessenden Behandeln mit NaNO2 in H2O
2: SOCl2
View Scheme
参考文献
Mann; Porter
Journal of the Chemical Society, 1945 , p. 751,757
反应条件
1: H2SO4 / anschliessenden Behandeln mit NaNO2 in H2O
2: SOCl2
View Scheme
参考文献
Mann; Porter
Journal of the Chemical Society, 1945 , p. 751,757
反应条件
1: H2SO4; H2O / Heating
2: SOCl2 / Heating
View Scheme
参考文献
Mann; Porter
Journal of the Chemical Society, 1945 , p. 751,757
反应条件
sodium hydroxide in methanol
2 h; Heating;
参考文献
Mukherjee; Kumar; Seth; Bhaduri
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 5 p. 391 - 396