2-亚甲基环己烷-1-醇合成路线 （共 70 条）
反应条件
in dimethyl sulfoxide
T=130°C; other ketones;
参考文献
Yurchenko, A. G.; Kirii, A. V.; Mel'nik, N. N.; Likhotvorik, I. R.; Zakharsh, P.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 10.2 p. 1925 - 1926
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 10 p. 2230 - 2231
反应条件
sodium dihydrogenphosphate; sodium nitrite
参考文献
Stapleford,K.S.J.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 2580 - 2582
反应条件
1: Py
2: aq. KOH / 150 - 160 °C
View Scheme
参考文献
Kovacs,E. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1962 , p. 116 - 122
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1962 , # 1 p. 130 - 138
反应条件
1: LiAlH4
2: NaNO2, aq. NaH2PO4
View Scheme
参考文献
Stapleford,K.S.J.
Journal of the Chemical Society [Section] C: Organic, 1971 , p. 2580 - 2582
反应条件
1: nBu3P, Py
2: aq. H2O2, Py
View Scheme
参考文献
Clive,D.L.J. et al.
Journal of the Chemical Society, Chemical Communications, 1978 , p. 770 - 771
反应条件
in dichloromethane
2 h; Ambient temperature;
参考文献
Sasaki, Kazuaki; Mori, Toshiharu; Doi, Yoshitaka; Kawachi, Akinori; Aso, Yoshio; et al.
Chemistry Letters, 1991 , # 3 p. 415 - 418
反应条件
lithium aluminium tetrahydride; oxygen
1) 60 grad C; Multistep reaction. Further byproducts given. Title compound not separated from byproducts;
参考文献
Blau, K.; Mueller, U.; Pritzkow, W.; Schmidt-Renner, W.; Sedshaw, Z.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 6 p. 915 - 932
反应条件
lithium aluminium tetrahydride; oxygen
1) 60 grad C; Multistep reaction. Further byproducts given. Title compound not separated from byproducts;
参考文献
Blau, K.; Mueller, U.; Pritzkow, W.; Schmidt-Renner, W.; Sedshaw, Z.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 6 p. 915 - 932
反应条件
lithium aluminium tetrahydride; oxygen
1) 60 grad C; Multistep reaction. Further byproducts given. Title compound not separated from byproducts;
参考文献
Blau, K.; Mueller, U.; Pritzkow, W.; Schmidt-Renner, W.; Sedshaw, Z.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 6 p. 915 - 932
反应条件
(i) aq. H2O2, MeOH, (ii) (pyrolysis); Multistep reaction;
参考文献
Tsuji,T. et al.
Bulletin of the Chemical Society of Japan, 1967 , vol. 40, # 10 p. 2338 - 2343
