4-正十二烷氧基苯甲酸甲酯合成路线 （共 14 条）
反应条件
1: aq. NaOH / methanol / Heating 2: SOCl2 / Heating View Scheme
参考文献
Ili, Monica; Bucos, Madalina; Dumitracu, Florea; Circu, Viorel
Journal of Molecular Structure, 2011 , vol. 987, # 1-3 p. 1 - 6
反应条件
1: LiAlH4 / tetrahydrofuran 2: thionyl chloride / CH2Cl2; dimethylformamide 3: 90 percent / K2CO3 / dimethylformamide / 70 °C 4: 98 percent / LiAlH4 / tetrahydrofuran / 1 h / 23 °C View Scheme
参考文献
Percec, Virgil; Dulcey, Andres; Peterca, Mihai; Ilies, Monica; Miura, Yoshiko; Edlund, Ulrica; Heiney, Paul A.
Australian Journal of Chemistry, 2005 , vol. 58, # 6 p. 472 - 482
反应条件
1: With potassium hydroxide in tetrahydrofuran; ethanol; water Reflux; 2: in tetrahydrofuran; ethanol; water T=20°C; Acidic aq. solution;
参考文献
Khairuddean, Melati; Twieg, Robert J.
Molecular Crystals and Liquid Crystals, 2009 , vol. 503, # 1 p. 3 - 31
反应条件
1: LiAlH4 / tetrahydrofuran 2: thionyl chloride / CH2Cl2; dimethylformamide 3: 90 percent / K2CO3 / dimethylformamide / 70 °C View Scheme
参考文献
Johansson, Gary; Percec, Virgil; Ungar, Goran; Abramic, Darija
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 4 p. 447 - 460
反应条件
1: 100 percent / LiAlH4 / tetrahydrofuran / 1 h / 20 °C 2: 100 percent / PBr3 / CHCl3 / 1 h / 20 °C View Scheme
参考文献
Girotto, Edivandro; Eccher, Juliana; Vieira, Andre A.; Bechtold, Ivan H.; Gallardo, Hugo
Tetrahedron, 2014 , vol. 70, # 20 p. 3355 - 3360
反应条件
potassium carbonate; sodium iodide in acetonitrile
24 h; Heating;
参考文献
Ahmed, Saleh A.; Tanaka, Mutsuo
Journal of Organic Chemistry, 2006 , vol. 71, # 26 p. 9884 - 9886
反应条件
caesium carbonate in methanol; water; N,N-dimethyl-formamide
T=25°C; 1 h;
参考文献
Pozsgay
Organic letters, 1999 , vol. 1, # 3 p. 477 - 479
参考文献
Hegmann, Torsten; Marx, Vanessa M.
Patent: US2011/62385 A1, 2011 ;
反应条件
1: potassium carbonate / dichloromethane; acetonitrile
2: potassium carbonate
View Scheme
参考文献
Hegmann, Torsten; Marx, Vanessa M.
Patent: US2011/62385 A1, 2011 ;
反应条件
1: potassium carbonate / dichloromethane; acetonitrile
2: potassium carbonate
View Scheme
参考文献
Hegmann, Torsten; Marx, Vanessa M.
Patent: US2011/62385 A1, 2011 ;
