1,1,1-三氟-4,4-二乙氧基-3-丁烯-2-酮合成路线 (共 6 条)
反应条件
in ethanol 24 h; Heating;
参考文献
Martins, Marcos A.P.; Pereira, Claudio M.P.; Zimmermann, Nilo E.K.; Cunico, Wilson; Moura, Sidnei; Beck, Paulo; Zanatta, Nilo; Bonacorso, Helio G.
Journal of Fluorine Chemistry, 2003 , vol. 123, # 2 p. 261 - 265
反应条件
cyclohexyl isonitrile
参考文献
Simonyan,L.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1977 , vol. 26, p. 1906 - 1910
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1977 , vol. 26, # 9 p. 2061 - 2065
反应条件
in toluene
1.) 0.5 h; 2.) 90-95 deg C, 3 h;
参考文献
Narsaiah, B.; Sivaprasad, A.; Venkataratnam, R. V.
Journal of Fluorine Chemistry, 1994 , vol. 66, # 1 p. 47 - 50
反应条件
in toluene
0.133333 h; Irradiation;
参考文献
Chandra Sheker Reddy; Shanthan Rao; Venkataratnam
Tetrahedron, 1997 , vol. 53, # 16 p. 5847 - 5854
反应条件
in toluene
1.) 0.5 h; 2.) 90-95 deg C, 3 h;
参考文献
Narsaiah, B.; Sivaprasad, A.; Venkataratnam, R. V.
Journal of Fluorine Chemistry, 1994 , vol. 66, # 1 p. 47 - 50
反应条件
<b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '103233', constants.ctx, '0')">pyridine</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '1731042', constants.ctx, '0')">chloroform</a> <br />T=0 - 20°C; 1 h; <br /> <br />
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GMBH; BOEHRINGER INGELHEIM PHARMA GMBH and CO. KG Patent: WO2007/67836 A2, 2007 ; Location in patent: Page/Page column 170-171 ;