7-甲基-4-氧代-4H-色烯-3-甲醛合成路线 (共 3 条)
反应条件
1: N,N-dimethyl-formamide With bis(trichloromethyl) carbonate in 1,2-dichloro-ethane
T=0 - 20°C;
2: 4-methyl-2-hydroxyacetophenone in 1,2-dichloro-ethane
T=0 - 20°C; 4.5 h; Further stages.;
参考文献
Su; Li; Zhao
Organic Preparations and Procedures International, 2007 , vol. 39, # 5 p. 495 - 502
反应条件
in potassium hydroxide; ethanol
3 h; Heating;
参考文献
Thakak, K.A.; Gill, C.H.
Journal of the Indian Chemical Society, 1984 , vol. 61, p. 550 - 552
反应条件
1: With pyridine
Knoevenagel condensation; Reflux;
2: With hydrogenchloride in water
T=20°C; pH=1; 0.5 h;
参考文献
Joshi, Ratnadeep S.; Mandhane, Priyanka G.; Badadhe, Pravin V.; Gill, Charansingh H.
Ultrasonics Sonochemistry, 2011 , vol. 18, # 3 p. 735 - 738