双(2,2,2-三氟乙基)胺合成路线 （共 6 条）
反应条件
hydrogen; palladium/alumina at 50-60°C; product isolated as CF3CH2NH2*HCl;
参考文献
Gmelin Handbook: F: PerFHalOrg.9, 7, page 50 - 101
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Meen; Wright
Journal of Organic Chemistry, 1954 , vol. 19, p. 391,399
反应条件
ammonia T=210°C; 96 h;
参考文献
Buerger, H.; Krumm, B.; Pawelke, G.
Journal of Fluorine Chemistry, 1989 , vol. 44, p. 147 - 154
反应条件
bis(2,2'-bipyridine)ruthenium(II)-nitrosyl-chloride hexafluorophosphate in acetonitrile T=20°C; 48 h; Product distribution; Further Variations:Solvents;
参考文献
Di Salvo, Florencia; Crespo, Alejandro; Estrin, Dario A.; Doctorovich, Fabio
Tetrahedron, 2002 , vol. 58, # 21 p. 4237 - 4244
反应条件
1: Bis(2,2,2-trifluoroethyl)amine With n-butyllithium in diethyl ether
1 h; cooling;
2: carbon disulfide in diethyl ether
T=0 - 20°C;
参考文献
Weinstein, Randy D.; Grotzinger, Laurel L.; Salemo, Patrick; Omiatek, Donna M.; Bessel, Carol A.
Journal of Chemical and Engineering Data, 2005 , vol. 50, # 6 p. 2088 - 2093
反应条件
hydrogenchloride; sodium nitrite
参考文献
Haszeldine; Mattinson
Journal of the Chemical Society, 1955 , p. 4172,4184
