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Ferrito; Borg; Eagles; Fenwick
Biomedical Mass Spectrometry, 1979 , vol. 6, # 11 p. 499 - 501
1: calyxamide A With hydrogenchloride; water T=110°C; 24 h; 2: methanol With hydrogenchloride in water T=100°C; 0.5 h; 3: trifluoroacetic anhydride in dichloromethane; water T=100°C; 0.0833333 h;
参考文献
Kimura, Miki; Wakimoto, Toshiyuki; Egami, Yoko; Tan, Karen Co; Ise, Yuji; Abe, Ikuro
Journal of Natural Products, 2012 , vol. 75, # 2 p. 290 - 294
1: calyxamide B With hydrogenchloride; water T=110°C; 24 h; 2: methanol With hydrogenchloride in water T=100°C; 0.5 h; 3: trifluoroacetic anhydride in dichloromethane; water T=100°C; 0.0833333 h;
参考文献
Kimura, Miki; Wakimoto, Toshiyuki; Egami, Yoko; Tan, Karen Co; Ise, Yuji; Abe, Ikuro
Journal of Natural Products, 2012 , vol. 75, # 2 p. 290 - 294
1: calyxamide A With ozone in methanol T=-78°C; 0.25 h; 2: With hydrogenchloride; water T=110°C; 24 h; 3: methanol; trifluoroacetic anhydride Further stages;
参考文献
Kimura, Miki; Wakimoto, Toshiyuki; Egami, Yoko; Tan, Karen Co; Ise, Yuji; Abe, Ikuro
Journal of Natural Products, 2012 , vol. 75, # 2 p. 290 - 294
1: calyxamide B With ozone in methanol T=-78°C; 0.25 h; 2: With hydrogenchloride; water T=110°C; 24 h; 3: methanol; trifluoroacetic anhydride Further stages;
参考文献
Kimura, Miki; Wakimoto, Toshiyuki; Egami, Yoko; Tan, Karen Co; Ise, Yuji; Abe, Ikuro
Journal of Natural Products, 2012 , vol. 75, # 2 p. 290 - 294