2-甲基-2-(3-氧代-丁基)-环己酮合成路线 (共 17 条)
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
参考文献
Gawley,R.E.
Synthesis, 1976 , p. 777 - 794
反应条件
boron trifluoride diethyl etherate; mercury(II) oxide; trichloroacetic acid in methanol
1) 70 deg C, 2) 20 deg C, 90 min;
参考文献
Grattan, T. J.; Whitehurst, J. S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 1 p. 11 - 18
反应条件
sodium ethanolate
T=-10°C; 6 h;
参考文献
Janaki, S.; Subba Rao, G. S. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 505 - 507
反应条件
formic acid; mercury(II) diacetate
3 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Negishi, Ei-ichi; Luo, Fen-Tair; Pecora Anthony J.; Silveira, Augustine
Journal of Organic Chemistry, 1983 , vol. 48, # 14 p. 2427 - 2430
反应条件
formic acid; mercury(II) diacetate
3 h; Yield given. Yields of byproduct given;
参考文献
Negishi, Ei-ichi; Luo, Fen-Tair; Pecora Anthony J.; Silveira, Augustine
Journal of Organic Chemistry, 1983 , vol. 48, # 14 p. 2427 - 2430
反应条件
formic acid; mercury(II) diacetate
3 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Negishi, Ei-ichi; Luo, Fen-Tair; Pecora Anthony J.; Silveira, Augustine
Journal of Organic Chemistry, 1983 , vol. 48, # 14 p. 2427 - 2430
反应条件
carbon dioxide; triethylamine; magnesium chloride
1.) MeCN, 12 h, 2.) MeCN-Et2O, 6 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Olsen, Richard S.; Fataftah, Zakaria A.; Rathke, Michael W.
Synthetic Communications, 1986 , vol. 16, # 10 p. 1133 - 1140