(三甲基硅基)乙酸乙酯合成路线 （共 118 条）
反应条件
LiN(Cy)2
1.) THF, -78 deg C, 15 min, 2.) THF, from -78 deg C to 25 deg C, 4.5 h; Yield given. Multistep reaction;
参考文献
Patel; Vyas; Pandey; Tavares; Fernandes
Synthetic Communications, 1991 , vol. 21, # 18-19 p. 1935 - 1940
反应条件
1:
2: With diisobutylaluminium hydride
Further stages.;
参考文献
Taguchi, Haruhiko; Ghoroku, Kazushi; Tadaki, Makoto; Tsubouchi, Akira; Takeda, Takeshi
Organic Letters, 2001 , vol. 3, # 23 p. 3811 - 3814
反应条件
tetrabutylammonium fluoride absorbed on silica gel in tetrahydrofuran
2 h; Ambient temperature;
参考文献
Gambacorta, Augusto; Turchetta, Stefano; Botta, Maurizio
Synthetic Communications, 1989 , vol. 19, # 13-14 p. 2441 - 2448
反应条件
n-butyllithium; N,N-dicyclohexylamine in tetrahydrofuran; hexane
1.) -78 deg C, 3 h, 2.) -25 deg C, 1 h;
参考文献
Dobner, B.; Nuhn, P.; Buege, A.; Burkhardt, U.
Pharmazie, 1984 , vol. 39, # 1 p. 21 - 22
反应条件
iodine cloride in tetrachloromethane
0.5 h; Ambient temperature;
参考文献
Bordeau, M.; Djamei, S. M.; Dunogues, J.
Bulletin de la Societe Chimique de France, 1986 , # 3 p. 413 - 417
参考文献
Gold; Sommer; Whitmore
Journal of the American Chemical Society, 1948 , vol. 70, p. 2875
反应条件
Ambient temperature;
参考文献
Bordeau, M.; Djamei, S. M.; Dunogues, J.
Bulletin de la Societe Chimique de France, 1986 , # 3 p. 413 - 417
参考文献
Gold; Sommer; Whitmore
Journal of the American Chemical Society, 1948 , vol. 70, p. 2874
