2-羟基-3-甲基二苯甲酮合成路线 （共 11 条）
反应条件
iron(III) chloride T=170°C; 24 h;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 7 p. 539 - 548
反应条件
aluminum oxide; methanesulfonic acid
T=160°C; 0.833333 h;
参考文献
Sharghi, Hashem; Kaboudin, Babak
Journal of Chemical Research, Miniprint, 1998 , # 10 p. 2678 - 2695
反应条件
aluminum oxide; methanesulfonic acid
T=140°C; 0.333333 h;
参考文献
Sharghi, Hashem; Kaboudin, Babak
Journal of Chemical Research, Miniprint, 1998 , # 10 p. 2678 - 2695
反应条件
1: SOCl2, pyridine / petroleum ether / 6 h / Heating
2: 1.) AlCl3 / 1.) 2 deg C, 2.) a) RT, overnight, b) reflux, 3.5 h
View Scheme
参考文献
Evans, Delme; Cracknell, Mark E.; Saunders, John C.; Smith, Christine E.; Williamson, W. R. Nigel; et al.
Journal of Medicinal Chemistry, 1987 , vol. 30, # 8 p. 1321 - 1327
反应条件
1.1: magnesium / diethyl ether / 1.5 h / Reflux
1.2: 2 h / 0 °C / Reflux
2.1: air; Mn3O4 nanoparticles / N,N-dimethyl-formamide / 6 h / 80 °C
View Scheme
参考文献
Sun, Huayin; Zhang, Yonghui; Guo, Fengfeng; Yan, Yizhe; Wan, Changfeng; Zha, Zhenggen; Wang, Zhiyong
European Journal of Organic Chemistry, 2012 , # 3 p. 480 - 483
反应条件
1.1: magnesium / diethyl ether / 1.5 h / Reflux
1.2: 2 h / 0 °C / Reflux
2.1: air; Mn3O4 nanoparticles / N,N-dimethyl-formamide / 6 h / 80 °C
View Scheme
参考文献
Sun, Huayin; Zhang, Yonghui; Guo, Fengfeng; Yan, Yizhe; Wan, Changfeng; Zha, Zhenggen; Wang, Zhiyong
European Journal of Organic Chemistry, 2012 , # 3 p. 480 - 483
反应条件
aluminium trichloride
参考文献
Reich; Nightingale
Journal of Organic Chemistry, 1956 , vol. 21, p. 825
反应条件
1: SOCl2 / 2 h / 50 °C
2: AlCl3 / 2 h / Heating
View Scheme
参考文献
Tomioka, Hideo; Kimoto, Kohji; Murata, Hiroshi; Izawa, Yasuji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 2 p. 471 - 477
反应条件
aluminium trichloride
2 h; Heating;
参考文献
Tomioka, Hideo; Kimoto, Kohji; Murata, Hiroshi; Izawa, Yasuji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 2 p. 471 - 477
反应条件
iron(III) chloride
T=170°C; 24 h;
参考文献
Martin, Robert; Lafrance, Jean Ronald; Demerseman, Pierre
Bulletin des Societes Chimiques Belges, 1991 , vol. 100, # 7 p. 539 - 548
