1,1,2,2,3,3,4,4-辛氟戊烷合成路线 （共 3 条）
反应条件
1: With titanium tetrachloride
Inert atmosphere;
2: With zinc in diethylene glycol dimethyl ether
T=90°C; 9 h; Cooling with ice;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY; STEPANOV, Andrei, Aleksandrovich; CHERSTKOV, Victor, Filippovich; NAPPA, Mario, Joseph
Patent: WO2011/90734 A1, 2011 ;
Location in patent: Page/Page column 6-7 ;
反应条件
tri-n-butyl-tin hydride
2 h; Heating;
参考文献
Puy, Michael Van Der; Belter, Randolph K.; Borowski, Ralph J.; Ellis, Lois A. S.; Persichini, Phillip J.; et al.
Journal of Fluorine Chemistry, 1995 , vol. 71, # 1 p. 59 - 64
反应条件
di-tert-butyl peroxide in benzene
T=130°C; 1 h;
参考文献
Gizatullina, S. P.; Sokolovskii, A. V.; Germash, A. V.; Zlot-skii, S. S.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. <2> 60, # 11 p. 2565 - 2568,2297 - 2299
