5’-O-(叔丁基二甲基甲硅烷基)胸苷合成路线 （共 23 条）
反应条件
copper(II) sulfate in xylene Heating;
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 27, # 8 p. 931 - 948
反应条件
copper(II) sulfate in xylene Heating;
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 27, # 8 p. 931 - 948
反应条件
Decaborane in tetrahydrofuran; methanol T=20°C; 6 h;
参考文献
Jeong, Yeon Joo; Lee, Ji Hee; Park, Eun Soo; Yoon, Cheol Min
Journal of the Chemical Society, Perkin Transactions 1, 2002 , # 10 p. 1223 - 1225
反应条件
copper(II) sulfate in xylene Heating;
参考文献
Cabral, Nadia L. D.; Thiessen, Luciano Hoeltgebaum; Doboszewski, Bogdan
Nucleosides, Nucleotides and Nucleic Acids, 2008 , vol. 27, # 8 p. 931 - 948
反应条件
copper(II) sulfate in xylene Heating;
参考文献
Cabral, Nadia L. D.; Thiessen, Luciano Hoeltgebaum; Doboszewski, Bogdan
Nucleosides, Nucleotides and Nucleic Acids, 2008 , vol. 27, # 8 p. 931 - 948
反应条件
1: toluene / 80 °C 2: AIBN / toluene / 80 °C 3: 59 percent / Br2 / CCl4 4: 77 percent / aq. KOH View Scheme
参考文献
Fiandor, Jose; Tam, Steve Y.
Tetrahedron Letters, 1990 , vol. 31, # 5 p. 597 - 600
反应条件
1: 8.80 g / dimethylformamide / 2.5 h / 80 °C 2: (n-Bu)3SnH; AIBN / dioxane / 7 h / Heating 3: 2.86 g / trifluoroacetic acid / dioxane; H2O / 4 h / 20 °C View Scheme
参考文献
Filichev, Vyacheslav V.; Vester, Birte; Pedersen, Erik B.
Bioorganic and Medicinal Chemistry, 2004 , vol. 12, # 11 p. 2843 - 2851
反应条件
1: azobisisobutyronitrile 2: triethylamine; HF View Scheme
参考文献
Chu, Chung K.; Doboszewski, B.; Schmidt, Walter; Ullas, Giliyar V.
Journal of Organic Chemistry, 1989 , vol. 54, # 11 p. 2767 - 2769
反应条件
1: pyridine / 24 h
2: tetrabutylammonium fluoride / tetrahydrofuran / 4 h
View Scheme
参考文献
Wang, Guangyi; Seifert, Wilfried E.
Tetrahedron Letters, 1996 , vol. 37, # 36 p. 6515 - 6518
反应条件
1.1: imidazole / dimethylformamide / 0.5 h / 0 °C
1.2: 78 percent / dimethylformamide / 15 h / 20 °C
2.1: 87 percent / HF / acetonitrile; H2O / 1 h / 20 °C
View Scheme
参考文献
Abbas, Sahar; Hayes, Christopher J.
Synlett, 1999 , # 7 p. 1124 - 1126
