5-碘-1,3-的甲基尿嘧啶合成路线 (共 19 条)
反应条件
ammonium cerium(IV) nitrate; iodine in acetonitrile T=80°C; 2.5 h; other reagents investigated;
参考文献
Asakura, Jun-ichi; Robins, Morris J.
Journal of Organic Chemistry, 1990 , vol. 55, # 16 p. 4928 - 4933
反应条件
sodium hydride in N,N-dimethyl-formamide 0.5 h; Ambient temperature;
参考文献
Matsuhashi, Hayao; Hatanaka, Yasuo; Kuroboshi, Manabu; Hiyama, Tamejiro
Heterocycles, 1996 , vol. 42, # 1 p. 375 - 384
反应条件
sodium hydroxide in water T=0 - 100°C; 2 h;
参考文献
Dziuba, Dmytro; Karpenko, Iuliia A.; Barthes, Nicolas P. F.; Michel, Benoit Y.; Klymchenko, Andrey S.; Benhida, Rachid; Demchenko, Alexander P.; Mely, Yves; Burger, Alain
Chemistry - A European Journal, 2014 , vol. 20, # 7 p. 1998 - 2009
反应条件
iodine; potassium iodide T=80°C; 0.5 h;
参考文献
Skulski, Lech; Kujawa, Anna; Kujawa, Tadeusz M.
Bulletin of the Polish Academy of Sciences, Chemistry, 1987 , vol. 35, # 11-12 p. 499 - 505
反应条件
iodine; potassium iodide T=80°C; 0.5 h;
参考文献
Skulski, Lech; Kujawa, Anna; Kujawa, Tadeusz M.
Bulletin of the Polish Academy of Sciences, Chemistry, 1987 , vol. 35, # 11-12 p. 499 - 505
反应条件
N-iodo-succinimide in ethanol; chloroform T=50°C; 1 h;
参考文献
Bakker, Cees N. M.; Kaspersen, Frans M.
Recueil: Journal of the Royal Netherlands Chemical Society, 1981 , vol. 100, # 7/8 p. 267 - 271
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; indium; tri-tert-butyl phosphine; lithium iodide in N,N-dimethyl-formamide T=100°C; 18 h; Inert atmosphere;
参考文献
Lee, Kooyeon; Kim, Hyunseok; Mo, Juntae; Lee, Phil Ho
Chemistry - An Asian Journal, 2011 , vol. 6, # 8 p. 2147 - 2157
反应条件
in water; acetonitrile 10 h; Ambient temperatureIrradiation;
参考文献
Saito, Isao; Ikehira, Hideyuki; Matsuura, Teruo
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5148 - 5153
参考文献
Saito, Isao; Ikehira, Hideyuki; Matsuura, Teruo
Heterocycles, 1985 , vol. 23, # 1 p. 206
反应条件
(PPh4)Pd in tetrahydrofuran 16 h; Heating;
参考文献
Synthesis, , # 2 p. 213 - 215