1-(4-异丙氧基苯基)乙酮合成路线 (共 11 条)
反应条件
potassium carbonate in acetonitrile T=70°C;
参考文献
BIOENERGENIX
Patent: US2012/277224 A1, 2012 ;
Location in patent: Page/Page column 76 ;
US 20120277224 A1
反应条件
potassium carbonate in acetone T=70°C; 8 h;
参考文献
KOWA COMPANY, LTD.
Patent: US2010/280013 A1, 2010 ;
Location in patent: Page/Page column 15 ;
反应条件
1: isopropyl alcohol With N-benzyl-trimethylammonium hydroxide 0.166667 h; Neat (no solvent); 2: 1-fluoro-4-acetyl-benzene T=70°C; 1.08333 h; Neat (no solvent);
参考文献
Meshram; Goud, P. Ramesh; Reddy, B. Chennakesava; Kumar, D. Aravind
Synthetic Communications, 2010 , vol. 40, # 14 p. 2122 - 2129
参考文献
Bradley; Robinson
Journal of the Chemical Society, 1926 , p. 2363
反应条件
1: AlCl3; CS2 2: methanol. NaOH View Scheme
参考文献
McCoubrey; Iyengar
Journal of the Chemical Society, 1951 , p. 3430,3432
参考文献
Profft
Chemische Technik (Leipzig, Germany), 1952 , vol. 4, p. 241,242
反应条件
carbon disulfide; aluminium trichloride
参考文献
Bradley; Robinson
Journal of the Chemical Society, 1926 , p. 2363
反应条件
nickel in ethanol 2 h; Heating; Product distribution;
参考文献
Cabiddu, Salvatore; Cerioni, Giovanni; Cocco, Maria Teresa; Maccioni, Antonio; Plumitallo, Antonio
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 135 - 139
参考文献
Bradley; Robinson
Journal of the Chemical Society, 1926 , p. 2363
反应条件
1: 59 percent / bromine / dioxane; diethyl ether / 2 h / 20 °C
2: 83 percent / AlCl3; borane*tert-butylamine / CH2Cl2 / 3 h / 0 °C
View Scheme
参考文献
Treu, Matthias; Jordis, Ulrich; Mereiter, Kurt
Heterocycles, 2001 , vol. 55, # 9 p. 1727 - 1735