1,5-二羟基-1,2,3,4-四氢萘合成路线 （共 11 条）
反应条件
sodium tetrahydroborate in methanol
参考文献
Amgen Inc.
Patent: US7361789 B1, 2008 ;
Location in patent: Page/Page column 41; 49 ;
US 7361789 B1
反应条件
boron tribromide in dichloromethane T=-78 - 20°C; 6.5 h;
参考文献
Banerjee; Poon; Laya; Azocar
Russian Journal of General Chemistry, 2003 , vol. 73, # 11 p. 1815 - 1820
反应条件
kieselguhr; ethanol; nickel T=120°C; P=55898.6 Torr; Hydrogenation;
参考文献
Hardegger; Redlich; Gal
Helvetica Chimica Acta, 1945 , vol. 28, p. 628,633
反应条件
Candida cylindracea lipase in hexane; butan-1-ol T=25°C; 72 h;
参考文献
Pedrocchi-Fantoni, Giuseppe; Servi, Stefano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 8 p. 1029 - 1034
反应条件
1: 98 percent / NaBH4 / ethanol / 12 h 2: NaH / toluene / 1 h / Heating 3: 55 percent / BBr3 / CH2Cl2 / 6.5 h / -78 - 20 °C View Scheme
参考文献
Banerjee; Poon; Laya; Azocar
Russian Journal of General Chemistry, 2003 , vol. 73, # 11 p. 1815 - 1820
反应条件
1: NaH / toluene / 1 h / Heating 2: 55 percent / BBr3 / CH2Cl2 / 6.5 h / -78 - 20 °C View Scheme
参考文献
Banerjee; Poon; Laya; Azocar
Russian Journal of General Chemistry, 2003 , vol. 73, # 11 p. 1815 - 1820
反应条件
tert.-butylhydroperoxide; zirconium tetra-n-propoxide in dichloromethane T=20°C; 18 h;
参考文献
Krohn, Karsten; Khanbabaee, Karamali; Rieger, Hagen
Chemische Berichte, 1990 , vol. 123, # 6 p. 1357 - 1364
反应条件
caesium carbonate in toluene 8 h; Heating;
参考文献
Carlsen, Per H.J.; Liberkova, Katerina; Harrex, Rachel; Roe, Johan
Acta Chemica Scandinavica, 1997 , vol. 51, # 3 p. 343 - 344
反应条件
caesium carbonate in toluene
8 h; Heating;
参考文献
Carlsen, Per H.J.; Liberkova, Katerina; Harrex, Rachel; Roe, Johan
Acta Chemica Scandinavica, 1997 , vol. 51, # 3 p. 343 - 344
反应条件
methanol; sodium
Kochen des Reaktionsgemisches mit Methyljodid;
参考文献
Hardegger; Redlich; Gal
Helvetica Chimica Acta, 1945 , vol. 28, p. 628,633
