sodium hydride in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=20°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
1: 56 percent / diethyl ether / 60 h / Ambient temperature
2: 2 percent / LiAlH4 / benzene / 0.75 h / 80 °C
View Scheme
参考文献
Blunt, John W.; Hartshorn, Michael P.; Soong, Lee Tin; Munro, Murray H. G.; Vannoort, Richard W.; Vaughan, John
Australian Journal of Chemistry, 1983 , vol. 36, # 7 p. 1387 - 1398