1-(2-烯丙基-3,6-二羟基苯基)乙烷-1-酮合成路线 （共 8 条）
反应条件
T=220°C; 0.5 h; in vacuo;
参考文献
Bruce, J. Malcolm; Roshan-Ali, Yusuf
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2677 - 2679
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=-78°C; 1 h; Title compound not separated from byproducts;
参考文献
Uno, Hidemitsu
Journal of Organic Chemistry, 1986 , vol. 51, # 3 p. 350 - 358
反应条件
1: 52 percent / K2CO3 / butan-2-one / 72 h / Heating
2: 36 percent / 2 h / 200 - 220 °C
View Scheme
参考文献
Marshall; Goodson; Cullinan; Swanson-Bean; Haisch; Rinkema; Fleisch
Journal of Medicinal Chemistry, 1987 , vol. 30, # 4 p. 682 - 689
参考文献
Maruyama; Matano
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 12 p. 3877 - 3885
参考文献
Maruyama; Matano
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 12 p. 3877 - 3885
参考文献
Green, Ivan R.; Hugo, Victor I.; Oosthuisen, Francois J.; Eeden, Nestor van; Giles, Robin G. F.
South African Journal of Chemistry, 1994 , vol. 48, # 1/2 p. 15 - 22
反应条件
in acetonitrile
dissolved acylquinone and allylstannane stood for 10 min under Ar; concentrated; column chromy. (silica gel); eluted (hexane/ether); NMR; IR; mass spectra; elem. anal.;
参考文献
Maruyama; Matano
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 12 p. 3877 - 3885
参考文献
Naruta, Yoshinori; Uno, Hidemitsu; Maruyama, Kazuhiro
Tetrahedron Letters, 1981 , vol. 22, # 51 p. 5221 - 5224
