(9ci)-1H-吲唑-1,3-二胺合成路线 （共 7 条）
反应条件
1.1: 0.2 g / methanol / 3 h / Heating 2.1: 99 percent / aq. HCl / 0.25 h / Heating 3.1: KOH / dimethylsulfoxide / 0.08 h 3.2: 70 percent / dimethylsulfoxide / 2 h / 20 °C View Scheme
参考文献
Dyablo; Pozharskii; Kuz'menko; Kolesnichenko
Chemistry of Heterocyclic Compounds, 2001 , vol. 37, # 5 p. 567 - 573
反应条件
1: 0.2 g / methanol / 3 h / Heating 2: 99 percent / aq. HCl / 0.25 h / Heating View Scheme
参考文献
Dyablo; Pozharskii; Kuz'menko; Kolesnichenko
Chemistry of Heterocyclic Compounds, 2001 , vol. 37, # 5 p. 567 - 573
反应条件
hydrogen; palladium on activated charcoal in methanol
T=40 - 45°C; 8 h;
参考文献
Dyablo; Pozharskii; Kuz'menko; Kolesnichenko
Chemistry of Heterocyclic Compounds, 2001 , vol. 37, # 5 p. 567 - 573
反应条件
sodium hydroxide; sodium hydroxylamine-O-sulfonate in ethanol
T=50 - 60°C; 1.33333 h;
参考文献
Dyablo; Pozharskii; Kuz'menko; Kolesnichenko
Chemistry of Heterocyclic Compounds, 2001 , vol. 37, # 5 p. 567 - 573
反应条件
1: 88 percent / H2 / 2 percent Pd/C / methanol / 3 h / 20 °C
2: 99 percent / aq. HCl / 0.25 h / Heating
3: 10 percent / aq. NH2OSO3Na; NaOH / ethanol / 1.33 h / 50 - 60 °C
View Scheme
参考文献
Dyablo; Pozharskii; Kuz'menko; Kolesnichenko
Chemistry of Heterocyclic Compounds, 2001 , vol. 37, # 5 p. 567 - 573
反应条件
1: 99 percent / aq. HCl / 0.25 h / Heating
2: 10 percent / aq. NH2OSO3Na; NaOH / ethanol / 1.33 h / 50 - 60 °C
View Scheme
参考文献
Dyablo; Pozharskii; Kuz'menko; Kolesnichenko
Chemistry of Heterocyclic Compounds, 2001 , vol. 37, # 5 p. 567 - 573
反应条件
chloroform
T=20°C; 720 h;
参考文献
Dyablo; Pozharskii; Kuz'menko; Kolesnichenko
Chemistry of Heterocyclic Compounds, 2001 , vol. 37, # 5 p. 567 - 573
