3-(4-甲氧基苯甲酰基)-2H-色烯-2-酮合成路线 （共 5 条）
反应条件
piperidine in ethanol
8 h; Reflux;
参考文献
PIERRE FABRE MEDICAMENT; Rabot, Rémi; Bedjeguelal, Karim; Kaloun, El Bachir; Schmitt, Philippe; Rahier, Nicolas; Mayer, Patrice; Fournier, Emmanuel
Patent: US2014/31362 A1, 2014 ;
Location in patent: Paragraph 0302; 0303; 0304; 0305 ;
反应条件
in 1,4-dioxane
3 h; Heating;
参考文献
Andreichikov, Yu. S.; Tokmakova, T. N.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 4 p. 796 - 800
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 4 p. 880 - 885
反应条件
indium(III) chloride
T=100°C; Neat (no solvent);
参考文献
Verma, Rajiv Kumar; Verma, Girijesh K.; Raghuvanshi, Keshav; Singh, Maya Shankar
Tetrahedron, 2011 , vol. 67, # 3 p. 584 - 589
反应条件
1: NaH / 1,2-dimethoxy-ethane; paraffin / 4 h / Heating
2: piperidine / ethanol / Heating
View Scheme
参考文献
Specht, Donald P.; Martic, Peter A.; Farid, Samir; ++
Tetrahedron, 1982 , vol. 38, # 9 p. 1203 - 1211
反应条件
1.1: sodium hydride / hexane; N,N-dimethyl-formamide; mineral oil / 20 °C
1.2: 2 h / 20 °C
2.1: indium(III) chloride / 100 °C / Neat (no solvent)
View Scheme
参考文献
Verma, Rajiv Kumar; Verma, Girijesh K.; Raghuvanshi, Keshav; Singh, Maya Shankar
Tetrahedron, 2011 , vol. 67, # 3 p. 584 - 589
