2-氯-5,5-二甲基-1,3,2-二氧磷杂环己烷 2-氧化物合成路线 (共 31 条)
反应条件
tetrachloromethane; triethylamine in chloroform
参考文献
Wagner, Sebastian; Rakotomalala, Muriel; Bykov, Yana; Walter, Olaf; Doering, Manfred
Heteroatom Chemistry, 2012 , vol. 23, # 2 p. 216 - 222
反应条件
cyanogen chloride in dichloromethane
72 h; Ambient temperature;
参考文献
Uznanski, B.; Stec, W. J.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 6 p. 1225 - 1235,1093 - 1102
反应条件
tert-butylhypochlorite
T=20°C; Product distribution;
参考文献
Harger, Martin J.P
Tetrahedron Letters, 2001 , vol. 42, # 38 p. 6749 - 6752
反应条件
tert-butylhypochlorite
T=20°C; Product distribution;
参考文献
Harger, Martin J.P
Tetrahedron Letters, 2001 , vol. 42, # 38 p. 6749 - 6752
反应条件
in dichloromethane
24 h; Ambient temperaturevar. reaction times; Product distribution;
参考文献
Uznanski, B.; Stec, W. J.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 6 p. 1225 - 1235,1093 - 1102
参考文献
Edmundson,R.S.
Tetrahedron, 1964 , vol. 20, p. 2781 - 2795
反应条件
water
T=50°C; Kinetics;
参考文献
Koh, Han Joong; Kang, Suk Jin; Kevill, Dennis N.
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 7 p. 1404 - 1415
参考文献
Koh, Han Joong; Kang, Suk Jin; Kevill, Dennis N.
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 7 p. 1404 - 1415
反应条件
benzenephosphonous acid; sodium hydride in tetrahydrofuran
T=20°C; Inert atmosphere; chemoselective reaction;
参考文献
Nycz
Polish Journal of Chemistry, 2009 , vol. 83, # 4 p. 589 - 594
参考文献
Mikolajczyk,M. et al.
Tetrahedron, 1972 , vol. 28, p. 3855 - 3865