2-氯-5,5-二甲基-1,3,2-二氧磷杂环己烷 2-氧化物合成路线 （共 31 条）
反应条件
water
T=50°C; Kinetics;
参考文献
Koh, Han Joong; Kang, Suk Jin; Kevill, Dennis N.
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 7 p. 1404 - 1415
反应条件
water
T=50°C; Kinetics;
参考文献
Koh, Han Joong; Kang, Suk Jin; Kevill, Dennis N.
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 7 p. 1404 - 1415
反应条件
water
T=50°C; Kinetics;
参考文献
Koh, Han Joong; Kang, Suk Jin; Kevill, Dennis N.
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 7 p. 1404 - 1415
反应条件
water
T=50°C; Kinetics;
参考文献
Koh, Han Joong; Kang, Suk Jin; Kevill, Dennis N.
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 7 p. 1404 - 1415
参考文献
DAIHACHI CHEMICAL INDUSTRY CO., LTD.
Patent: EP1925622 A1, 2008 ;
Location in patent: Page/Page column 19 ;
反应条件
in diethyl ether
T=8 - 10°C;
参考文献
Sobkowska, Anna; Sobkowski, Michall; Cieslak, Jacek; Kraszewski, Adam; Kers, Inger; Stawinski, Jacek
Journal of Organic Chemistry, 1997 , vol. 62, # 14 p. 4791 - 4794
反应条件
1: in tetrahydrofuran
T=-78°C;
2: With sulfur in tetrahydrofuran
T=-33°C; 0.5 h;
参考文献
Stankiewicz, Marek; Nycz, Jacek; Rachon, Janusz
Heteroatom Chemistry, 2002 , vol. 13, # 4 p. 330 - 339
反应条件
benzenephosphonous acid; sodium hydride in tetrahydrofuran
T=20°C; Inert atmosphere; chemoselective reaction;
参考文献
Nycz
Polish Journal of Chemistry, 2009 , vol. 83, # 4 p. 589 - 594
反应条件
in toluene
T=25°C; Yields of byproduct given;
参考文献
Vijjulatha; Praveen Kumar; Kumara Swamy; Vittal
Tetrahedron Letters, 1998 , vol. 39, # 13 p. 1819 - 1822
反应条件
benzenephosphonous acid; sodium hydride in tetrahydrofuran
T=20°C; Inert atmosphere; chemoselective reaction;
参考文献
Nycz
Polish Journal of Chemistry, 2009 , vol. 83, # 4 p. 589 - 594
