[二[(三氟甲基)磺酰基]甲基]苯合成路线 (共 6 条)
反应条件
lithium hexamethyldisilazane in tetrahydrofuran T=-78 - 20°C; 6 h; Inert atmosphere;
参考文献
ABBOTT LABORATORIES; ABBOTT LABORATORIES TRADING (SHANGHAI) COMPANY, LTD.; WANG, Xueqing; MEYER, Michael; YAO, Betty; GUO, Tao; WEI, Guo Ping,Robert; WANG, Lijuan, Jane
Patent: WO2013/10453 A1, 2013 ;
Location in patent: Page/Page column 101 ;
反应条件
in tetrahydrofuran; diethyl ether
参考文献
Koshar,R.J.; Mitsch,R.A.
Journal of Organic Chemistry, 1973 , vol. 38, p. 3358 - 3363
参考文献
Hasegawa, Aiko; Ishikawa, Takuo; Ishihara, Kazuaki; Yamamoto, Hisashi
Bulletin of the Chemical Society of Japan, 2005 , vol. 78, # 8 p. 1401 - 1410
参考文献
Zhu, Shi-zheng; Chen, Qing-yun
Journal of the Chemical Society, Chemical Communications, 1990 , # 20 p. 1459 - 1460
反应条件
1: 94 percent / propiononitrile / Heating
View Scheme
参考文献
Hasegawa, Aiko; Ishikawa, Takuo; Ishihara, Kazuaki; Yamamoto, Hisashi
Bulletin of the Chemical Society of Japan, 2005 , vol. 78, # 8 p. 1401 - 1410
反应条件
2: 76 percent / 0.17 h / Heating
View Scheme
参考文献
Zhu, Shi-Zheng
Journal of Fluorine Chemistry, 1993 , vol. 64, # 1-2 p. 47 - 60