N-苯基-N-乙烯基乙酰胺合成路线 (共 5 条)
反应条件
potassium in 1,4-dioxane
T=160°C; P=9120 - 10640 Torr; 16 h;
参考文献
Afonin, A. V.; Trofimov, B. A.; Malysheva, S. F.; Vashchenko, A. V.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 2.1 p. 181 - 190
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 2 p. 225 - 236
反应条件
copper(l) iodide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in tetrahydrofuran
T=80°C; Inert atmosphere;
参考文献
Feltenberger, John B.; Hayashi, Ryuji; Tang, Yu; Babiash, Eric S.C.; Hsung, Richard P.
Organic Letters, 2009 , vol. 11, # 16 p. 3666 - 3669
反应条件
potassium in 1,4-dioxane
T=150°C; P=9120 Torr; 10 h; in autoclave;
参考文献
Trofimov, B. A.; Malysheva, S. F.; Vyalykh, E. P.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 1405 - 1409
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 8 p. 1583 - 1587
反应条件
potassium in 1,4-dioxane
T=150°C; P=9120 Torr; 2 h; other solvent; other temperature; other time; Product distributionMechanism;
参考文献
Trofimov, B. A.; Malysheva, S. F.; Vyalykh, E. P.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 1405 - 1409
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 8 p. 1583 - 1587
参考文献
Du Pont de Nemours and Co.
Patent: US2231905 , 1939 ;