4-(甲基磺酰基)苯甲酰氯合成路线 （共 26 条）
反应条件
1: 84 percent / pyridine / 3 h 2: 90 percent / LiBH4, cc. HCl / bis-(2-methoxy-ethyl) ether / 3 h 3: 48percent HBr, cc. sulfuric acid / 6 h / Heating View Scheme
参考文献
Brembilla, Alain; Roizard, Denis; Schoenleber, Jacqueline; Lochon, Pierre
Canadian Journal of Chemistry, 1984 , vol. 62, p. 2330 - 2336
反应条件
benzene Erhitzen einer Loesung des Reaktionsprodukts in Benzol mit wss. HCl und Essigsaeure;
参考文献
Fuller; Tonkin; Walker
Journal of the Chemical Society, 1945 , p. 633,639
反应条件
1: 79 percent Chromat. / HCOONH4 / Ru3(CO)12 / dioxane / 20 h / 160 °C View Scheme
参考文献
Chatani; Tatamidani; Ie; Kakiuchi; Murai
Journal of the American Chemical Society, 2001 , vol. 123, # 20 p. 4849 - 4850
反应条件
benzene Behandeln des Reaktionsprodukts mit methanol. Natriummethylat;
参考文献
Forrest; Walker
Journal of the Chemical Society, 1948 , p. 1506
反应条件
1: 84 percent / pyridine / 3 h 2: 90 percent / LiBH4, cc. HCl / bis-(2-methoxy-ethyl) ether / 3 h View Scheme
参考文献
Brembilla, Alain; Roizard, Denis; Schoenleber, Jacqueline; Lochon, Pierre
Canadian Journal of Chemistry, 1984 , vol. 62, p. 2330 - 2336
反应条件
thionyl chloride in N,N-dimethyl-formamide
4 h; Heating;
参考文献
Brembilla, Alain; Roizard, Denis; Schoenleber, Jacqueline; Lochon, Pierre
Canadian Journal of Chemistry, 1984 , vol. 62, p. 2330 - 2336
参考文献
Hinks; Jeremy David; Takle; Andrew Kenneth; Hunt; Eric
Patent: US6020368 A1, 2000 ;
反应条件
1: KMnO4, aq. NaOH
2: SOCl2 / tetrahydrofuran
View Scheme
参考文献
Chodnekar; Blum
Journal of medicinal chemistry, 1968 , vol. 11, # 5 p. 1023 - 1028
反应条件
1: aqueous sulfuric acid / 190 °C
2: thionyl chloride
View Scheme
参考文献
Fuller; Tonkin; Walker
Journal of the Chemical Society, 1945 , p. 633,639
反应条件
1: aqueous hydrochloric acid
2: sodium nitrite; aqueous hydrochloric acid / Eintragen der erhaltenen Suspension in eine warme, aus Nickel(II)-chlorid, Kaliumcyanid und Wasser hergestellte Loesung
3: aqueous sulfuric acid / 190 °C
4: thionyl chloride
View Scheme
参考文献
Fuller; Tonkin; Walker
Journal of the Chemical Society, 1945 , p. 633,639
