4-(甲基磺酰基)苯甲酰氯合成路线 (共 26 条)
反应条件
1: 84 percent / pyridine / 3 h
2: 90 percent / LiBH4, cc. HCl / bis-(2-methoxy-ethyl) ether / 3 h
3: 48percent HBr, cc. sulfuric acid / 6 h / Heating
4: thiourea / H2O / 12 h / 100 °C / Heating
View Scheme
参考文献
Brembilla, Alain; Roizard, Denis; Schoenleber, Jacqueline; Lochon, Pierre
Canadian Journal of Chemistry, 1984 , vol. 62, p. 2330 - 2336
参考文献
Buu-Hoi; Lecocq
Bulletin de la Societe Chimique de France, 1946 , p. 139,142
反应条件
1: Py
2: aq. NaOH / ethanol / 4.5 h / Ambient temperature
View Scheme
参考文献
Dunwell,D.W. et al.
Journal of Medicinal Chemistry, 1975 , vol. 18, # 1 p. 53 - 58
参考文献
Dunwell,D.W. et al.
Journal of Medicinal Chemistry, 1975 , vol. 18, # 1 p. 53 - 58
参考文献
Brembilla, Alain; Roizard, Denis; Schoenleber, Jacqueline; Lochon, Pierre
Canadian Journal of Chemistry, 1984 , vol. 62, p. 2330 - 2336
参考文献
Shirai et al.
Bl. Nagoya City Univ. pharm. SchoolChem.Abstr., 1954 , vol. 2, p. 45,47
Bl. Nagoya City Univ. pharm. SchoolChem.Abstr., 1956 , p. 11337