2-氨基-5-甲氧基苯酚合成路线 (共 31 条)
反应条件
nitrogen; palladium monocarbide in methanol
参考文献
Arvanitis, Argyrios G.; Gilligan, Paul J.; Hartz, Richard A.
Patent: US2003/171380 A1, 2003 ;
US 20030171380 A1
反应条件
hydrogen; palladium 10 on activated carbon in ethyl acetate
参考文献
KHAMRAI, Uttam; Ronsheim, Matthew; Karak, Sumit Kumar
Patent: US2010/152160 A1, 2010 ;
Location in patent: Page/Page column 54 ;
US 20100152160 A1
反应条件
1: glacial acetic acid; sodium nitrite / 0 °C 2: tin dichloride; hydrochloric acid View Scheme
参考文献
Hoshi-Sakoda; Usui; Ishizuka; Kosemura; Yamamura; Hasegawa
Phytochemistry, 1994 , vol. 37, # 2 p. 297 - 300
反应条件
1: HNO3 / propionic acid / 1.) 0 deg C, 1 h, 2.) from 0 deg C to RT, 2 h 2: potassium formate / 5percent Pd/C / ethanol / 3 h / 70 °C View Scheme
参考文献
Henrich; Rhodius
Chemische Berichte, 1902 , vol. 35, p. 1480
Full Text Show Details
Henrich; Eisenach
Journal fuer Praktische Chemie (Leipzig), 1904 , vol. <2>70, p. 332,334 Anm.2
反应条件
T=210 - 215°C; 1.5 h;
参考文献
Nishioka, Hiromi; Ohmori, Yukiko; Iba, Yumiko; Tsuda, Eri; Harayama, Takashi
Heterocycles, 2004 , vol. 64, p. 193 - 198
反应条件
hydrogenchloride; tin(ll) chloride
参考文献
Bechhold
Chemische Berichte, 1889 , vol. 22, p. 2382
反应条件
trifluoroacetic acid T=37°C; 4.5 h; ΔH(excit.), ΔG(excit.), ΔS(excit.); Product distributionRate constantKinetics;
参考文献
Haga, Naoki; Endo, Yasuyuki; Kataoka, Ken-Ichiro; Yamaguchi, Kentaro; Shudo, Koichi
Journal of the American Chemical Society, 1992 , vol. 114, # 25 p. 9795 - 9806
反应条件
sodium dithionite; water in dimethyl sulfoxide T=20°C; pH=7.4; phosphate buffer; Kinetics;
参考文献
Leriche, Geoffray; Budin, Ghyslain; Brino, Laurent; Wagner, Alain
European Journal of Organic Chemistry, 2010 , # 23 p. 4360 - 4364
反应条件
1: KOH-solution 2: tin dichloride; hydrochloric acid View Scheme
参考文献
Henrich; Birkner
Chemische Berichte, 1913 , vol. 46, p. 3380
参考文献
Henrich; Rhodius
Chemische Berichte, 1902 , vol. 35, p. 1480
Full Text Show Details
Henrich; Eisenach
Journal fuer Praktische Chemie (Leipzig), 1904 , vol. <2>70, p. 337