对乙酰氨基-邻甲氧基苯甲酸甲酯合成路线 (共 45 条)
反应条件
platinum (IV)-chloride in 1,4-dioxane T=55°C; 18 h;
参考文献
Stevenson, Neil G.; Curtis, Neil R.; Northall, John M.; Gray, Matthew; Prodger, Jeremy C.; Walker, Andrew J.
Organic Process Research and Development, 2010 , vol. 14, # 1 p. 92 - 98
反应条件
1: nickel-aluminium-alloy; aq. NaOH solution 2: sulfuric acid 3: chloroform View Scheme
参考文献
Drain et al.
Journal of the Chemical Society, 1949 , p. 1498,1502
反应条件
in 2-methyl tetrahydrofuran T=75°C; 18 h;
参考文献
Stevenson, Neil G.; Curtis, Neil R.; Northall, John M.; Gray, Matthew; Prodger, Jeremy C.; Walker, Andrew J.
Organic Process Research and Development, 2010 , vol. 14, # 1 p. 92 - 98
反应条件
1: platinum; ethanol / Hydrogenation 2: chloroform View Scheme
参考文献
Drain et al.
Journal of the Chemical Society, 1949 , p. 1498,1502
参考文献
Drain et al.
Journal of the Chemical Society, 1949 , p. 1498,1502
参考文献
Hueckel; Janecka
Archiv der Pharmazie (Weinheim, Germany), 1951 , vol. 284, p. 341,346
参考文献
Drain et al.
Journal of the Chemical Society, 1949 , p. 1498,1502
反应条件
1: 95.5 percent / K2CO3, tetra-n-butylammonium chloride / acetonitrile / 22 h / Heating 2: 94.9 percent / N-methylpyrrolidone / 1.5 h / Heating View Scheme
参考文献
Kakigami, Takuji; Usui, Toshinao; Tsukamoto, Katsura; Kataoka, Tadashi
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 1 p. 42 - 52
反应条件
1: 98.4 percent / K2CO3 / dimethylformamide / 24 h / 20 - 30 °C 2: NCS / dimethylformamide / 3 h / 70 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 46, # 1 p. 42 - 52
反应条件
1: sodium hydroxide / N,N-dimethyl-formamide 2: N-bromosuccinmide / N,N-dimethyl-formamide 3: sodium hydroxide / ethanol View Scheme
参考文献
Deng, Xin; Zhao, Xinxin; Han, Jing; Wang, Jingjie; Huang, Wenlong; Qian, Hai; Ge, Liang
Letters in Drug Design and Discovery, 2012 , vol. 9, # 5 p. 489 - 493