1-叠氮基-2,4-二硝基苯合成路线 (共 23 条)
反应条件
sodium azide; (C16H33)Bu3P(1+)*N3(1-) in water; chlorobenzene
T=25°C;
参考文献
Landini, Dario; Maia, Angelamaria; Montanari, Fernando
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 461 - 466
反应条件
sodium azide in methanol; water
T=25°C; pH 8.00 to 10.00, ionic strength of 0.1 mol l-1; Rate constant;
参考文献
Zima, Vitezslav; Pytela, Oldrich; Vecera, Miroslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 4 p. 814 - 821
反应条件
Et4NN3 in acetonitrile
T=19.9°C; other temperature (298 K, 303 K, 323 K), activation enthalpy, activation entropy; Rate constantThermodynamic data;
参考文献
Sinev, V. V.; Plokhikh, G. V.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 10 p. 1973 - 1978
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 10 p. 2155 - 2161
反应条件
Et4NN3 in acetonitrile
T=19.9°C; other temperature (298 K, 303 K, 323 K), activation enthalpy, activation entropy; Rate constantThermodynamic data;
参考文献
Sinev, V. V.; Plokhikh, G. V.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 10 p. 1973 - 1978
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 10 p. 2155 - 2161
反应条件
sodium azide; QN3 in water; chlorobenzene
T=25°C; various temp.; Rate constant;
参考文献
Landini, Dario; Maia, Angelamaria; Montanari, Fernando
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 461 - 466
反应条件
1: sulfuric acid; nitric acid / 3 h / 100 - 105 °C
2: sodium azide / acetonitrile / 20 h / 20 °C
View Scheme
参考文献
Zaitsev; Vatsadze; Dalinger; Kachala; Nelyubina; Shevelev
Russian Chemical Bulletin, 2009 , vol. 58, # 10 p. 2109 - 2117
反应条件
sodium azide; QN3 in water; chlorobenzene
T=25°C; various temp.; Rate constant;
参考文献
Landini, Dario; Maia, Angelamaria; Montanari, Fernando
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 461 - 466
参考文献
Luetgert
Chemische Berichte, 1957 , vol. 70, p. 151,156
反应条件
T=20°C; 168 h; PhotolysisNeat (no solvent);
参考文献
Leyva, Elisa; Gonzalez-Balderas, Regina M.; De Loera, Denisse A.; Jimenez-Catano, Rogelio
Tetrahedron Letters, 2012 , vol. 53, # 19 p. 2447 - 2449
参考文献
Drost
Justus Liebigs Annalen der Chemie, 1899 , vol. 307, p. 49
Full Text Show Details
Noelting; Kohn
Chemiker-Zeitung, Chemische Apparatur, 1894 , vol. 18, p. 1095