2-甲氧羰基琥珀酸二甲酯合成路线 （共 19 条）
反应条件
carbon dioxide 1) CH3CN, room temp, platinum-anode, plumbum-cathode; Multistep reaction;
参考文献
Engels, Rainer; Smit, Cornelis J.; Tilborg, Wim J. M. van
Angewandte Chemie, 1983 , vol. 95, # 6 p. 502 - 503
反应条件
in diethyl ether T=0°C; 1 h; var. methylcopper reagents, further quenching with D2O-DCl, <13C>-labelled; Product distributionMechanism;
参考文献
Chounan, Yukiyasu; Ibuka, Toshiro; Yamamoto, Yoshinori
Journal of the Chemical Society, Chemical Communications, 1994 , # 17 p. 2003 - 2004
反应条件
potassium carbonate in dimethyl sulfoxide Ambient temperature;
参考文献
Tou, Jacob S.; Schleppnik, Alfred A.
Journal of Organic Chemistry, 1983 , vol. 48, # 5 p. 753 - 755
反应条件
1: sodium methylate / methanol / 0 - 25 °C / Inert atmosphere 2: trichlorophosphate 3: ammonia / methanol / 6 h / 60 °C 4: carbon / ethyl acetate / 1 h / Reflux View Scheme
参考文献
Vaid, Radhe K.; Spitler, Jeremy T.; Boini, Sathish; May, Scott A.; Hoying, Richard C.
Synthesis (Germany), 2012 , vol. 44, # 15 p. 2396 - 2400
反应条件
1: sodium methylate / methanol / 0 - 25 °C / Inert atmosphere 2: trichlorophosphate 3: ammonia / methanol / 6 h / 60 °C View Scheme
参考文献
Vaid, Radhe K.; Spitler, Jeremy T.; Boini, Sathish; May, Scott A.; Hoying, Richard C.
Synthesis (Germany), 2012 , vol. 44, # 15 p. 2396 - 2400
反应条件
1: sodium methylate / methanol / 0 - 25 °C / Inert atmosphere 2: trichlorophosphate 3: ammonia / butan-1-ol / 12 h / 95 °C View Scheme
参考文献
Vaid, Radhe K.; Spitler, Jeremy T.; Boini, Sathish; May, Scott A.; Hoying, Richard C.
Synthesis (Germany), 2012 , vol. 44, # 15 p. 2396 - 2400
反应条件
1: sodium methylate / methanol / 0 - 25 °C / Inert atmosphere 2: trichlorophosphate 3: ammonia / isopropyl alcohol / 6 h / 100 °C View Scheme
参考文献
Vaid, Radhe K.; Spitler, Jeremy T.; Boini, Sathish; May, Scott A.; Hoying, Richard C.
Synthesis (Germany), 2012 , vol. 44, # 15 p. 2396 - 2400
反应条件
1: sodium methylate / methanol / 0 - 25 °C / Inert atmosphere
2: trichlorophosphate
View Scheme
参考文献
Vaid, Radhe K.; Spitler, Jeremy T.; Boini, Sathish; May, Scott A.; Hoying, Richard C.
Synthesis (Germany), 2012 , vol. 44, # 15 p. 2396 - 2400
反应条件
sodium hydroxide
2.) cation-exchange chromatography; Yield given. Multistep reaction;
参考文献
Christy, M. Robert; Koch, Tad H.
Journal of the American Chemical Society, 1982 , vol. 104, # 6 p. 1771 - 1772
