反应条件
1: 1.) N-methylmorpholine, 2-(1H-benzotriazol-1-yl)-1,1,3,3-tetramethyluronium tetrafluoroborate / 1.) DMF, room temperature, 20 min, 2.) DMF, room temperature, 18 h
2: 65 percent / hydrogen, glacial acetic acid / Pd on carbon / ethanol; H2O / 18 h
View Scheme
参考文献
Rai, Bijaya L.; Khodr, Hicham; Hider, Robert C.
Tetrahedron, 1999 , vol. 55, # 4 p. 1129 - 1142